4.4 Article

Post-Annealing Influence on Magnetic Properties of Rapidly Quenched Ni-Mn-Ga Glass-Coated Microwires

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IEEE TRANSACTIONS ON MAGNETICS
卷 57, 期 7, 页码 -

出版社

IEEE-INST ELECTRICAL ELECTRONICS ENGINEERS INC
DOI: 10.1109/TMAG.2021.3076395

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Annealing; glass-coated microwires; magnetic properties; rapid solidification; stress relaxation

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In this study, the impact of post-annealing process on the magnetic properties of Ni-Mn-Ga microwires was investigated, revealing the significant influence of crystallographic structure and internal stresses on the magnetic properties.
In this article, we showed how the post-annealing process affects the magnetic properties of rapidly quenched Ni-Mn-Ga glass-coated microwires. Microwires with Ni63Mn12Ga25 chemical composition, total diameter D = 54.6 mu m and metallic nucleus diameter d = 26.7 mu m, were prepared by the Taylor-Ulitovsky technique. The annealing temperature was fixed at 873 K, and the time was 1 and 10 h. The microwires were slowly cooled to room temperature after annealing. Based on thermomagnetic curves and hysteresis loops, we suggest crystallographic texture in the wires that considerably affect magnetic properties. The wires' internal structure indicates nanocrystalline state with radial micrometers and submicrometer grains distribution in the wire annealed during 10 h. A ferromagnetic-to-paramagnetic phase transition occurs around room temperature. No signs of a martensitic transformation were found. The difference in magnetization saturation, remanence, and Curie temperature values for 1- and 10-h annealed microwires indicates the influence of internal stresses and that created by the presence of a glass coating.

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