期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 363, 期 14, 页码 3481-3484出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.202100329
关键词
ring expansion; thermal conditions; cyclopropyl azide; one-pot reaction; heterocycles
An efficient and systematic synthesis of 1-pyrrolines from cyclobutyl azides under thermal and neutral conditions is reported. The reaction generates nitrogen as the sole by-product and the 1-pyrrolines can be further transformed into other compounds in one-pot manner.
We herein report an efficient and systematic synthesis of 1-pyrrolines from cyclobutyl azides under thermal and neutral conditions. The reaction proceeded without any additional reagents, and nitrogen was generated as the sole by-product. Furthermore, the generated 1-pyrrolines could be continuously transformed into pyrroles, N-Boc-amines, and oxaziridines in an one-pot manner.
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