4.6 Article

A Micro-Computed Tomography Comparison of the Porosity in Additively Fabricated CuCr1 Alloy Parts Using Virgin and Surface-Modified Powders

期刊

MATERIALS
卷 14, 期 8, 页码 -

出版社

MDPI
DOI: 10.3390/ma14081995

关键词

computed tomography; porosity analysis; surface-modified CuCr1 powder; laser powder-bed fusion; additive manufacturing; laser reflectivity

资金

  1. EU Framework Programme for Research and Innovation-Horizon 2020-Grant within the PAM2 (precision additive metal manufacturing) research project [721383]
  2. Agentschap Innoveren en Ondernemen (VLAIO) [150010]

向作者/读者索取更多资源

This study compares dense specimens produced from virgin and surface-modified CuCr1 powder, as well as characterizes a third sample with abnormal porosity content. High-resolution micro-CT scans reveal that the virgin CuCr1 sample has keyhole pores and pit cavities, while the surface-modified sample mainly contains small and spherical equi-distributed metallurgical defects. The presence of W contamination in the third specimen leads to lack-of-fusion pores in subsequent LPBF layers. The different porosity types are connected to the LPBF melting mode, material properties, and potential contaminants.
Recently, the use of novel CuCr1 surface-modified powder for reliable laser powder-bed fusion (LPBF) manufacturing has been proposed, enabling a broader LPBF processing window and longer powder storage life. Nevertheless, virgin CuCr1 powder is also LPBF processable, on the condition that a high-energy density is employed. In this work, we compare two dense specimens produced from virgin and surface-modified CuCr1 powder. Furthermore, a third sample fabricated from surface-modified powder is characterized to understand an abnormal porosity content initially detected through Archimedes testing. Utilizing high-resolution micro-CT scans, the nature of the defects present in the different samples is revealed. Pores are analyzed in terms of size, morphology and spatial distribution. The micro-CT data reveal that the virgin CuCr1 dense specimen displays keyhole pores plus pit cavities spanning multiple layer thicknesses. On the other hand, the sample fabricated with the surface-modified CuCr1 powder mainly contains small and spherical equi-distributed metallurgical defects. Finally, the CT analysis of the third specimen reveals the presence of a W contamination, favoring lack-of-fusion pores between subsequent LPBF layers. The LPBF melting mode (keyhole or conductive), the properties of the material, and the potential presence of contaminants are connected to the different porosity types and discussed.

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