期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2016, 期 33, 页码 5539-5544出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201600962
关键词
Synthesis design; Aromatic substitution; Cross-coupling; Azulenes; Carbocycles; Cyclization
资金
- University of Helsinki
- Magnus Ehrnrooth Foundation
An efficient synthetic route to 1,3,6-trisubstituted azulenes based on the 1-acyloxyazulene scaffold was developed. The 1-position in azulene was substituted in the ring-formation step with a functionalized acyloxy group. Additionally, the 3- and 6-positions of azulene were functionalized with versatile synthetic handles, a halogen atom and a formyl group.
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