4.7 Article

A quasi in-situ EBSD study of the nucleation and growth of Goss grains during primary and secondary recrystallization of a strip-cast Fe-6.5 wt% Si alloy

期刊

JOURNAL OF ALLOYS AND COMPOUNDS
卷 861, 期 -, 页码 -

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2020.158550

关键词

Grain-oriented Fe-6.5 wt% Si alloy; Strip casting; Quasi in-situ EBSD; Goss texture; Primary recrystallization; Secondary recrystallization

资金

  1. National Natural Science Foundation of China [51974085, 51674080]
  2. National Key R&D Program of China [2017YFB0304105, 2017YFB0304400]
  3. Natural Resources Canada through the Program of Energy Research and Development
  4. Chinese Scholarship Council [201806080099]

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The research investigated the nucleation and growth of Goss grains during primary and secondary recrystallization of a strip-cast grain-oriented Fe-6.5 wt% Si alloy using a quasi in situ electron backscatter diffraction (EBSD) technique. It was found that Goss grains nucleated from shear bands during primary recrystallization tend to survive during subsequent grain growth. Abnormally growing Goss grains were observed at the surfaces when the primary recrystallization temperature increased to 850 degrees C, consuming the entire thickness during secondary recrystallization. Using a classical grain growth model, the abnormal growth of Goss grains during secondary recrystallization could be roughly predicted.
The nucleation and growth of Goss grains during primary and secondary recrystallization of a strip-cast grain-oriented Fe-6.5 wt% Si alloy were investigated using a quasi in situ electron backscatter diffraction (EBSD) technique. During primary recrystallization at 700 degrees C, the Goss was found to nucleate from two locations in the deformed < 111 >//ND (normal direction) grains: in the shear bands and at the grain boundaries. However, only those nucleated from the shear bands tended to survive during the subsequent grain growth. Even the survived Goss grains would not develop as abnormal Goss grains during secondary recrystallization. Abnormally growing Goss grains were formed at the surfaces when the primary recrystallization temperature was 850 degrees C, which grew into the center and consumed the entire thickness during secondary recrystallization. The abnormal growth of the Goss grains was attributed to the large fraction of 20-45 degrees grain boundaries at the growing front, which essentially did not change during secondary recrystallization. Using a classical grain growth model, the migration velocities of Goss grains during abnormal growth were calculated, which were compared to the experimental migration velocities obtained from the quasi in situ EBSD data. It was shown that the model could roughly predict the abnormal growth of the Goss grains during secondary recrystallization.

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