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ORGANIC LETTERS
卷 23, 期 4, 页码 1484-1488出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.1c00189
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An efficient photoredox system based on decatungstate/disulfide catalysts was developed for the hydrofunctionalization of styrenes. The use of disulfide as a cocatalyst was crucial for enhancing reaction efficiency, allowing for the synthesis of a wide variety of useful building blocks and high-value molecules from simple starting materials, such as amides and unsymmetrical ketones.
We describe an efficient photoredox system, relying on decatungstate/disulfide catalysts, for the hydrofunctionalization of styrenes. In this methodology the use of disulfide as a cocatalyst was shown to be crucial for the reaction efficiency. This photoredox system was employed for the hydro-carbamoylation, -acylation, -alkylation, and -silylation of styrenes, giving access to a large variety of useful building blocks and high-value molecules such as amides and unsymmetrical ketones from simple starting materials.
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