4.3 Article

A new SOLARIS beamline optimized for X-ray spectroscopy in the tender energy range

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ELSEVIER
DOI: 10.1016/j.nimb.2020.12.017

关键词

Tender-energy X-ray spectroscopy; X-ray beamline; X-ray crystals; National Synchrotron Radiation Centre; SOLARIS

资金

  1. Innovative Hochschule - Leuchtturm NR - Aus der Hohe in die Breite by Federal Ministry of Education and Research, Germany [03-IHS-084]
  2. EU Horizon2020 program [952148-Sylinda]

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The new X-ray absorption spectroscopy beamline at the National Synchrotron Radiation Centre SOLARIS has a fixed exit beam Lemmonier type monochromator, allowing the coverage of the desired energy range with different crystal sets. It is a high vacuum system, enabling quick crystal changes and minimizing photon absorption.
A new X-ray absorption spectroscopy (XAS) beamline is currently under construction at a bending magnet of the National Synchrotron Radiation Centre SOLARIS. The front end of this beamline was installed in April 2020. This beamline has a few outstanding characteristic features: The monochromator is a fixed exit beam Lemmonier type monochromator allowing to cover the pursued energy range (1 keV to similar to 15 keV) with 3 sets of crystals: KAP (100) + multilayer, InSb (111) and Ge (220). The monochromator is a high vacuum system allowing the change of crystals in less than an hour. In order to minimize absorption of photons no windows will be installed in the beamline down to the monochromator, and just one thin polypropylene window will be used for separating the vacuum of the monochromator from the ionization chambers and the sample chamber. A special differential ion pump will be installed to maintain the pressure difference of four orders of magnitude between the storage ring and the monochromator. As SOLARIS is a low energy machine, the beamline can be built without any radiation safety hutches without exceeding the strict low radiation safety levels. The straightforward design of the beamline without additional optical elements, its compact overall dimensions and an easy to handle monochromator make this beamline especially user friendly. In combination with the characteristics of the 1.5 GeV SOLARIS storage ring this beamline will be specifically attractive for the tender X-ray range, i.e. the K-edges of important elements such as P, S, Si, Al and Mg.

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