4.7 Article

Direct evidence for stress-induced face-centered cubic zirconium

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ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2021.140814

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Zircaloy-4 alloy; Stress-induced; Phase transformation; Face-centered cubic structure; EBSD technique

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The direct evidence of stress-induced face-centered cubic (FCC) zirconium was reported for the first time using in-situ electron backscatter diffraction (EBSD) and indentation observation. Two orientation relations (OR) (B-type and P type) between hexagonal close-packed (HCP) and FCC phases were detected, with the rotation axis and angle identified as [101] and 52.1 degrees, respectively. Mechanisms of HCP -> FCC phase transformation involve partial dislocation gliding theory and shuffle displacement.
The direct evidence for stress-induced face-centered cubic (FCC) zirconium was firstly reported using in-situ electron backscatter diffraction (EBSD) and indentation observation. The transformed FCC phases governed by a high stress (1244.92 MPa) induced by a load of 500 g. Two orientation relations (OR) (including B-type and P type) between the hexagonal close-packed (HCP) and FCC phase were both detected. The mechanisms of HCP -> FCC phase transformation were proposed by follows: B-type OR was achieved via partial dislocation gliding theory, while P-type OR was attained through the partial dislocation gliding and shuffle displacement. Moreover, the interface between B-type and P-type FCC phase was identified as (110) plane and the rotation axis and angle were [101] and 52.1 degrees, respectively.

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