期刊
ELECTROCHIMICA ACTA
卷 220, 期 -, 页码 164-168出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.electacta.2016.10.066
关键词
hydrothermal synthesis; LiFePO4; iron metal; cathode; lithium-ion batteries
资金
- Ministry of Science and Technology in Taiwan [NSC 102-2628-M-110-001-MY3]
Hydrothermal LiFePO4 has been successfully synthesized using iron powder as an iron source and as an in situ reducing agent. The 100% atom economy delivered by iron metal (Fe-0) makes this process green and inexpensive. A plausible mechanism for the formation of hydrothermal LiFePO4 powder is also proposed. The structure of the LiFePO4 powder is well characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy techniques. The discharge capacity of the LiFePO4 electrode is found to be 165 mAhg(-1) at 0.1 C-rate, and the cycle-life performance is comparable to the conventionally synthesized LiFePO4. (c) 2016 Elsevier Ltd. All rights reserved.
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