期刊
CHEMISTRYSELECT
卷 5, 期 46, 页码 14534-14537出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/slct.202003999
关键词
o-cyanoarylacrylamides; cyclization; quinolone-2; 4-dione; radical reaction; thiols
资金
- National Natural Science Foundation of China [21761132021]
- Jiangsu Qin Lan Project
- open project of chemistry department of Qingdao University of Science and Technology [QUSTHX202005]
A radical cascade sulfuration/cyclization of o-cyanoarylacrylamides with dicumyl peroxide as an oxidant and thiols as coupling partners has been developed. This reaction was conducted under simple conditions and showed wide substrate scope, affording the corresponding products in good chemical yields. This work provides a new and efficient strategy for the preparation of 3-thiomethylated quinoline-2,4-diones.
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