期刊
JOURNAL OF APPLIED CRYSTALLOGRAPHY
卷 54, 期 -, 页码 371-375出版社
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600576720014776
关键词
sample cell; pressure; temperature; powder diffraction
资金
- Research Council of Norway under the Frinatek Program [250728]
A sample cell for powder X-ray diffraction studies with in situ applied pressure and temperature control system is demonstrated. The cell is easily portable to synchrotron facilities and commissioning tests were performed in a custom-made small/wide-angle X-ray diffractometer at the Norwegian University of Science and Technology. The temperature control system mainly focuses on achieving temperature control between -30 and 200 degrees Celsius.
A sample cell for powder X-ray diffraction studies with in situ applied pressure and control of temperature is demonstrated. The cell is based on a previously reported design and consists of a glass or quartz capillary glued into a Swagelok weld gland; this configuration can hold up to 100 bar (1 bar = 100 kPa). The cell is placed in contact with a copper plate for control of temperature between -30 and 200 degrees C. This is achieved by Peltier elements, heat cartridges and a refrigerated circulating bath. This work mainly focuses on the temperature control system. Commissioning tests were performed in a custom-made small/ wide-angle X-ray diffractometer at the Norwegian University of Science and Technology. The system is easily portable to synchrotron facilities.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据