Hot deformation mechanisms, mechanical properties and microstructural evolution of a HP-Nb steel

In this study hot deformation mechanisms, mechanical properties and microstructural evolution of a HP-Nb steel used as reformers tube in oil and gas industries was examined. Hot tensile tests were performed on the as-cast samples in temperature range from 700 degrees C to 1000 degrees C with 100 degrees C interval and under various strain rates. Microstructural analyses of the hot tensile samples were performed using optical microscope and Field Emission Scanning Microscope (FE-SEM). Constitutive equations were constructed to define deformation regimes. In that regard, and based on apparent activation energy, strain rate sensitivity and Zener-Hollomon parameters were calculated. Results showed that increasing temperature after 800 degrees C substantially reduced the flow stress. Such an effect was a little offset by increasing the strain rate. Strain rate sensitivity was remarkably increased at 800 degrees C and again at 1000 degrees C which indicated an increase in ductility due to the occurrence of dynamic recrystallization (DRX) at these temperatures. Strain rate sensitivity was relatively low at 700 degrees C and 900 degrees C with the latter being higher than 700 degrees C. It was seen that increasing the deformation temperature to 900 degrees C led to a decrease in the possibility of DRX due mainly to strain induced precipitation (SIP) and solute drag effect of Nb element. It was also observed that increasing the engineering strain rate from 0.002 s(-1) significantly increased the flow stress due probably to the domination of work hardening over restoration phenomena, particularly at 700 degrees C. As well, it was found that when deformation temperature increased, particularly at lower strain rate regimes, more dynamically recrystallized grains were developed. A contour map of Zener-Hollomon parameter together with the strain rate and temperature is constructed which defined the deformation regime under various combinations of strain rates and temperatures.

Automated summary

The study investigated the hot deformation mechanisms, mechanical properties, and microstructural evolution of a HP-Nb steel used in reformers tubes for oil and gas industries. Results showed that increasing temperature reduced flow stress and increasing strain rate offset this effect. Dynamic recrystallization was observed at 800°C and 1000°C, leading to increased ductility. Increasing deformation temperature to 900°C decreased the possibility of dynamic recrystallization, primarily due to strain-induced precipitation and solute drag of Nb element.