期刊
CURRENT NANOSCIENCE
卷 17, 期 6, 页码 886-892出版社
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/1573413716666201207141117
关键词
FeCo nanoparticles; chemical reduction process; polyethylene glycol [PEG 200]; cubes; high magnetization; bio-sensors; drug delivery
类别
资金
- National Research Foundation of Korea (NRF) - Korean government [2019R1H1A2079946, 2020R1A2C100613611]
- National Research Council of Science and Technology (NST) - Korea government (MSIT) [CRC-15-06-KIGAM]
- National Research Foundation of Korea [2019R1H1A2079946] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
Controlled morphological FeCo nanoparticles with different Fe/Co ratios were prepared by a surfactant-free modified chemical reduction process in the water medium. The shape of FeCo nanoparticles varied from flakes to cubes according to the atomic ratio of the metal precursors. Among all samples, Fe60Co40 had the highest magnetization of 208 emu/g according to the vibrating Sample Magnetometer (VSM) measurements.
Objective: Controlled morphological FeCo nanoparticles with different Fe/Co ratios were prepared by a surfactant-free modified chemical reduction process in the water medium. Methods: Polyethylene glycol PEG 200 was used to protect from areal oxidation of FeCo alloy, and a mixture of hydrazine, sodium hydroxide was served as the reducing system in this process. Results: It was found that the shape of FeCo nanoparticles varied from flakes to cubes according to the atomic ratio of the metal precursors. X-ray diffraction (XRD) data showed that the prepared samples with different compositions got a single-phase body-centered-cubic structured FeCo alloy. Scanning Electron Microscopy (SEM) and transmission electron microscopy (TEM) confirmed all sample's atomic ratios and sizes (FeCo cubes with a size of similar to 130 nm). Conclusion: The vibrating Sample Magnetometer (VSM) measurements reveal that the Fe60Co40 had the highest magnetization of 208 emu/g among all samples.
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