期刊
SYNLETT
卷 31, 期 19, 页码 1919-1924出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0040-1705948
关键词
flow reaction; gas-liquid reaction; hydrogenation; alkynes; alkenes; phenols
资金
- JSPS KAKENHI [JP15H03844, JP18H02012]
- MEXT KAKENHI [JP18H04397]
We describe a promising method for the continuous hydrogenation of alkenes or alkynes by using a newly developed fine-bubble generator. The fine-bubble-containing slug-flow system was up to 1.4 times more efficient than a conventional slug-flow method. When applied in the hydrogenation of phenols to the corresponding cyclohexanones, the fine bubble-slug-flow method suppressed over-reduction. As this method does not require the use of excess gas, it is expected to be widely applicable in improving the efficiency of gas-mediated flow reactions.
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