期刊
CRYSTENGCOMM
卷 18, 期 10, 页码 1752-1759出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ce02097b
关键词
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资金
- National Natural Science Foundation of China [51205276, 51205275, 51205274, 61474079]
- China Postdoctoral Science Foundation [2013T60268]
- Science and Technology Major Project of the Shanxi Science and Technology Department [20121101004]
- Shanxi Province Science Foundation for Youths [2012021021-5, 2013021017-1]
- Shanxi Province Foundation for Returnees [2013-036]
In this work, uniform single-crystalline alpha-Fe2O3 concave and hollow nanocrystals have been synthesized by a facile top-down etching method. Phosphate ions were employed as an etching agent to etch pristine icositetrahedra along their [006] direction in a top-down manner. The etched Fe2O3 concave and hollow nanocrystals exhibit a much larger specific surface area (SSA) and more edges, corners and rough structures (hot spots) on the crystal surface compared to their mother crystal, thus serving as the possible origin of their comparative photocatalytic activities in the degradation of cationic dye Rhodamine B. These characteristics make them promising candidates as catalysts and sensing materials.
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