期刊
ORGANIC LETTERS
卷 22, 期 18, 页码 7244-7249出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c02574
关键词
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资金
- Cooperative Research Program of the Institute for Catalysis, Hokkaido University [19B1019]
- JSPS KAKENHI [JP 18H04260, T15K149760, T15KT00630]
- Platform Project for Supporting Drug Discovery and Life Science Research (Basis for Supporting Innovative Drug Discovery and Life Science Research (BINDS)) from AMED [JP20am0101084]
- Cooperative Research Program of the Network Joint Research Center for Materials and Devices from the Ministry of Education, Culture, Sports, Science and Technology (MEXT)
- Nagase Science Technology Foundation
Self-assembled multilayer iron(0) nanoparticles (NPs, 6-10 nm), namely, sulfur-modified Au-supported Fe(0) [SAFe(0)], were developed for ligand-free one-pot carbon-carbon/carbon-nitrogen bond-forming reactions. SAFe(0) was successfully prepared using a well-established metal-nanoparticle catalyst preparative protocol by simultaneous in situ metal NP and nanospace organization (PSSO) with 1,4-bis(trimethylsilyl)-1,4-dihydropyrazine (Si-DHP) as a strong reducing agent. SAFe(0) was easy to handle in air and could be recycled with a low iron-leaching rate in reaction cycles.
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