期刊
CHEMISTRY OF HETEROCYCLIC COMPOUNDS
卷 56, 期 8, 页码 1054-1061出版社
SPRINGER
DOI: 10.1007/s10593-020-02773-7
关键词
acetone-1,3-dicarboxylates; aminotriazoles; dihydropyrido[3,4-e]triazolo[1,5-a]pyrimidines; dimethylformamide dimethyl acetal; 1,2,4-triazolo[1,5-a]pyrimidines; high-resolution HPLC/MS; multicomponent reactions
资金
- Russian Science Foundation [18-74-10097]
- Russian Science Foundation [18-74-10097] Funding Source: Russian Science Foundation
A new multicomponent reaction for regioselective synthesis of substituted 1,2,4-triazolo[1,5-a]pyrimidines using aminotriazoles, beta-ketoglutaric acid dimethyl ester, and dimethylformamide dimethyl acetal was implemented. The selective reduction of 1,2,4-triazolo-[1,5-a]pyrimidines to dihydro derivatives and the use of triazolo pyrimidines as starting compounds in multicomponent synthesis of dihydropyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidinecarboxylates was demonstrated.
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