期刊
INTERNATIONAL JOURNAL OF APPLIED CERAMIC TECHNOLOGY
卷 17, 期 6, 页码 2629-2637出版社
WILEY
DOI: 10.1111/ijac.13592
关键词
lightweight aggregate; microporous magnesia-based refractory; original salt pseudomorph; pore size distribution; Thermal conductivity
资金
- National Natural Science Foundation of China [51772139]
In recent years, there was a huge demand for basic lightweight insulation materials in the metallurgical industry, especially magnesia-based refractories with low thermal conductivity. Therefore, the preparation of microporous magnesia-based refractory products through the synthesis of lightweight aggregate and the different grain compositions to meet the supply of light basic refractories is discussed in this paper. The microstructure, pore size distribution, phase composition, coefficient of thermal expansion, thermal conductivity and sintering properties of the microporous magnesia-based refractory products sintered at 1600 degrees C were characterized. The results indicated that the original salt pseudomorph produced by the thermal decomposition of magnesite fine powder (porogenic agent) provides a uniform microporous structure for the synthesis of lightweight aggregates. The microporous morphology of the periclase phase was controlled by adjusting the content of the porogenic agent. The average pore size of microporous magnesia-based refractory ranged from 1.5 to 4.2 mu m, and the apparent porosity increased from 29.88% to 32.46%. In the same time, the thermal conductivity increased from 0.037 to 0.217 W/(m K), indicating that the introduction of homologous porogenic agents could produce lightweight alkaline refractories with high porosity and low thermal conductivity.
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