期刊
CATALYSTS
卷 10, 期 5, 页码 -出版社
MDPI
DOI: 10.3390/catal10050491
关键词
metal-to-metal charge transfer; Nb2O5; catalytic decolorization; dyes; water purification
资金
- Ministry of Science, ICT and Future Planning of Korea [2020R1H1A1003814, NRF-2017R1C1B1002851]
- Cooperative R&D between Industry, Academy, and Research Institute funded Korea Ministry of SMEs and Startups in 2019 [S2652595]
- Korea Science Academy of KAIST
- Ministry of Science and ICT
- Korea Technology & Information Promotion Agency for SMEs (TIPA) [S2652595] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
- National Research Foundation of Korea [2020R1H1A1003814] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
In this work, a new metal-to-metal charge transfer (MMCT) heterogeneous catalyst (Nb-O-Mo) was synthesized by a chemical grafting method under an inert atmosphere. The activity of the covalently anchored oxo-bridged Nb-O-Mo catalyst was estimated for decolorization of Rh B, congo red, and crystal violet dyes in an aqueous solution under fluorescent light. The catalyst was characterized via X-ray diffraction, scanning electron microscopy with energy-dispersive X-ray spectrometer, Fourier-transform infrared, and FT-Raman. The catalytic decolorization was evaluated from the UV spectra of dyes in aqueous solution by changing different factors, including dye concentration, temperature, and catalyst loading. Decolorization percentages were 83%-89%, 86%-95%, 97%-99% for Rh B, Congo Red and Crystal Violet in 1 min at 298 K, showing the best performance among other catalysts. Decolorization efficiency for 50 ppm of Rh B was improved from 92% to 98%, with a temperature increase to 318 K.
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