期刊
CHEMISTRY OF MATERIALS
卷 29, 期 1, 页码 90-105出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.chemmater.6b02726
关键词
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资金
- BASF (SE) through Academic Battery and Electrochemistry International Network
- BASF (Canada) through Academic Battery and Electrochemistry International Network
- Joint Centre for Energy Storage Research, a Hub - Department of Energy, USA
- NSERC
- Natural Resources Canada
- Waterloo Institute for Nanotechnology
- Ontario Government
We present an overview of the procedures and methods to prepare and evaluate materials for electrochemical cells in battery research in our laboratory, including cell fabrication, two- and three-electrode cell studies, and methodology for evaluating diffusion coefficients and impedance measurements. Informative characterization techniques employed to assess new materials for batteries are also described, including operando XRD, pair-distribution function analysis, X-ray photoelectron spectroscopy, and operando X-ray absorption spectroscopy. Examples of insightful information that each technique has provided in the research areas of Li-S, Na-ion, and Mg batteries are presented along with excellent references for detailed descriptions of the theory, experimental procedures, and various designs, as well as methods for data processing and analysis.
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