期刊
CHEMISTRY OF MATERIALS
卷 28, 期 11, 页码 4072-4081出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.chemmater.6b01796
关键词
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资金
- Deutsche Forschungsgemeinschaft [PO 1744/1-1]
- IMPRS Functional Interfaces in Physics and Chemistry
- Einstein Foundation Berlin by an Einstein-Junior-Fellowship [EJF-2011-95]
- BMBF [FKZ 03EK3009]
This contribution investigates the growth mechanism of the Turkevich method. The experimental results provide the missing piece of the mechanistic puzzle which enables the actual control of particle growth in the commonly used Turkevich method. Applying the gained knowledge, the boundary conditions for a successful Turkevich synthesis are deduced. Moreover, the conditions under which the Turkevich method is highly reproducible are derived. Following these conditions, the Turkevich synthesis is modified to reveal small monodisperse particles with an unprecedented reproducibility of +/- 0.1 nm.
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