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A new neutron depth profiling spectrometer at the JCNS for a focused neutron beam

期刊

RADIATION EFFECTS AND DEFECTS IN SOLIDS
卷 175, 期 3-4, 页码 342-355

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TAYLOR & FRANCIS LTD
DOI: 10.1080/10420150.2019.1701466

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Neutron depth profiling; in situ; operando methods; near-surface analysis; thin-film lithium batteries

资金

  1. Grant Agency of the Czech Republic [18-07619S]

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A new neutron depth profiling (NDP) spectrometer has been designed and built for the use at a high intensity focused cold neutron beam of the reflectometer MARIA at the Heinz Maier-Leibnitz Zentrum (MLZ, Germany). The extremely high neutron flux at the sample position of MARIA joined with the multiple charged particle detectors allows less than 10 s sampling rate and paves the way to study the kinetics of Li ions in thin-film microbatteries. The performance of the spectrometer with standard calibration samples and amorphous thin films is presented; possibilities to operando study the Li distribution inside thin-film rechargeable lithium batteries are discussed.

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