期刊
ORGANIC LETTERS
卷 22, 期 11, 页码 4213-4216出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c01264
关键词
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资金
- Max Planck Society
A pressure-based variable-bed flow reactor built for peptide synthesis and capable of real-time monitoring of resin swelling was adapted for automated glycan assembly. In the context of the solid-phase synthesis of several oligosaccharides, the coupling efficiencies, resin growth patterns, and saccharide solvation during the synthesis were determined. The presented work provides the first estimation of on-resin oligosaccharide solvation and an alternative technique to UV-vis monitoring.
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