期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 142, 期 11, 页码 5002-5006出版社
AMER CHEMICAL SOC
DOI: 10.1021/jacs.0c00359
关键词
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资金
- Indiana University
- NIH [R01GM110131, R35GM131755]
- Vice Provost for Research through the Research Equipment Fund
- NSF [CHE1726633]
The first enantioselective synthesis of (-)-cajanusine is presented. Key features of the route include a rapid synthesis of the [4.2.0]bicyclooctane core by an enantioselective isomerization/stereoselective [2+2]-cycloaddition strategy as well as prominent use of catalytic methods for bond construction. The evolution of the approach is also presented that highlights unexpected roadblocks and how novel solutions were developed.
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