期刊
CHEMICAL COMMUNICATIONS
卷 52, 期 57, 页码 8846-8849出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc05147b
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资金
- Engineering and Physical Sciences Research Council (EPSRC) [EP/E052789/1]
- Department of Chemistry, University College London
- Pfizer (EPSRC CASE award)
- GlaxoSmithKline
- EPSRC [EP/E052789/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/E052789/1, 1353678] Funding Source: researchfish
A commercially available borate ester, B(OCH2CF3)(3), can be used to achieve protecting-group free direct amidation of alpha-amino acids with a range of amines in cyclopentyl methyl ether. The method can be applied to the synthesis of medicinally relevant compounds, and can be scaled up to obtain gram quantities of products.
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