期刊
APPLIED SURFACE SCIENCE
卷 510, 期 -, 页码 -出版社
ELSEVIER
DOI: 10.1016/j.apsusc.2020.145431
关键词
Cobalt oxide; Citric acid; Open-hollow spheres; Li-ion battery; Cycling stability
类别
资金
- CONACYT-SENER [274314]
- U.S. Office of Naval Research (ONR) [N00014-16-1-2465]
Co3O4 open hollow structures were synthesized by a new green alternative of Pechini method that implies three simple steps: (i) an initial formation of Co2+- citric soluble coordination compounds, (ii) hydrothermal processing (180 degrees C) in the presence of fructose followed by (iii) air thermal processing of the as-obtained precursor. Benefiting from its exclusive structural features, this appealing hollow Co3O4 material demonstrated superior specific capacity, rate performance and cycling stability (specific capacity of 848 mA h g(-1) at an applied C-rate of 0.5 C with a coulombic efficiency of 98% after 250 cycles) in comparison with multi-shelled hollow spheres obtained in the absence of citric acid (525 mA h g(-1) with a coulombic efficiency of 97% recorded under the same conditions).
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