期刊
ASIAN JOURNAL OF ORGANIC CHEMISTRY
卷 9, 期 2, 页码 218-221出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ajoc.201900726
关键词
Guanidine; Spirocyclization; Dearomatization; Hypervalent iodine; keyword 5
资金
- A3-foresight program
- SUNBOR
- Japan Society for the Promotion of Science (JSPS), KAKENHI [18K14210]
- [18H04387]
- [JP26282214]
- Grants-in-Aid for Scientific Research [18K14210] Funding Source: KAKEN
We have developed a versatile synthetic method for the construction of spirocyclic guanidines in moderate yields by intramolecular dearomative oxidative cyclization of guanidino phenols using the hypervalent iodine reagent 4-chloro-1-(diacetoxyiodo)benzene in 2,2,3,3-tetrafluoro-1-propanol.
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