期刊
TETRAHEDRON LETTERS
卷 61, 期 12, 页码 -出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2020.151648
关键词
Hf(OTf)(4); (RS)(2)/(RSe)(2); C-1-S/Se; C-3-S/Se glycal; Ferrier Rearrangement
资金
- National Natural Science Foundation of China (NSFC) [21272305]
By using Hf(OTf)(4) as the catalyst, under certain conditions, reaction of tri-O-acetyl-D-glucal and ((2R,3S)-3-acetoxy-2,3-dihydrofuran-2-yl)methyl acetate with alkyl(aryl) bisulfide/alkyl(aryl) biselenide as nucleophile precursor leads to temperature-dependent formation of C-1-S/Se and C-3-S/Se product. A temperature-dependent profile of the yield of these two products is given. (C) 2020 Elsevier Ltd. All rights reserved.
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