期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 64, 期 13, 页码 1681-1686出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023619130084
关键词
UHTC; ultra-high-temperature material; high-enthalpy air flow; induction plasmatron
资金
- Council for Grants of the President of the Russian Federation [MD-5535.2018.3]
- Russian Foundation for Basic Research [17-01-00054-a]
Samples of an ultra-high-temperature HfB2-30 vol % SiC ceramic material with an SiC crystallite size of 50 nm have been fabricated by hot pressing of an HfB2-(SiO2-C) composite powder synthesized through a sol-gel route. It has been found that the selected hot-pressing conditions (1800 degrees C, 15 min, 30 MPa) ensure complete conversion of silica to silicon carbide and afford a material with a relative density of 96.9%. The effect of a relief applied to the sample surface in the form of ring grooves with a depth of <0.5 mm on the oxidation of the material exposed to a subsonic dissociated air flow-temperature distribution over the surface, elemental and phase composition, and microstructure-has been studied using a high-frequency induction plasmatron.
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