期刊
REVIEW OF SCIENTIFIC INSTRUMENTS
卷 91, 期 1, 页码 -出版社
AMER INST PHYSICS
DOI: 10.1063/1.5124301
关键词
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资金
- MAXNET Energy
- University of Virginia
- DOE Office of Science [DE-SC0012704]
A high-throughput, operando-ready X-ray absorption spectroscopy catalytic reaction cell consisting of 4 parallel reactors was designed to collect X-ray absorption near edge structure and extended fine structure spectra under reaction conditions. The cell is capable of operating at temperatures from ambient conditions up to 773 K and pressures from ambient to 2 MPa in a variety of gas environments. The cell design is mechanically simple, and programmable operation at beamline 8-ID (NSLS-II, Brookhaven National Laboratory) makes it straightforward to use. Reactor tube parts were available as-fabricated from commercial sources, while the heating jacket and cell mounting required custom machining. Published under license by AIP Publishing.
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