期刊
ORGANIC LETTERS
卷 22, 期 5, 页码 1818-1824出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00139
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-
资金
- Russian Foundation for Basic Research [18-33-00693]
Sulfonylated N-unsubstituted enamines were synthesized through a chain of chemical and electrochemical transformations via sulfonylation of vinyl azides. The disclosing of the N-unsubstituted enamines synthesis was based on a unique property of the azido group, which is its ability to eliminate the N-2 molecule. Furthermore, a formal paradox is observed: a double bond reacts and a double bond is retained. Electrosynthesis proceeded in an undivided cell equipped with a graphite anode and a stainless steel cathode; NH4I was used as a supporting electrolyte.
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