期刊
ORGANIC LETTERS
卷 22, 期 5, 页码 1908-1913出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00255
关键词
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资金
- Indian Institute of Technology (ITT) Patna
An expeditious approach has been developed for the synthesis of succinimide-fused unsymmetrical 9,10-dihydrophenanthrenes from simple aryl iodides and maleimides. The developed transformation, overall proceeding with high regioselectivity via a cascade approach through palladium(II)-catalyzed Micheal-type addition/C-H activation/intramolecular cross-dehydrogenative coupling (ICDC)/C-H activation, allows formation of four fundamental carbon-carbon bonds in one-pot fashion. The reactions tolerate broad functional groups and satisfy the parameters of atom and step economy. Detailed mechanistic studies were carried out to support the proposed synthetic pathway.
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