期刊
ORGANIC LETTERS
卷 22, 期 5, 页码 1889-1893出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00227
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资金
- Chinese Scholarship Council
A new methodology for the carbonylative transformation of N-fluoro-sulfonamides into N-sulfonyl-beta-homoproline esters has been described. In the presence of a catalytic amount of Cu(OTf)(2), a range of beta-homoproline derivatives were prepared in moderate to good yield. The reaction proceeds via the intramolecular cyclization and intermolecular carbonylation of a free carbon radical. Notably, this procedure offers the possibility to build potential functionalized bioactive molecules.
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