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ORGANIC LETTERS
卷 22, 期 4, 页码 1580-1584出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.0c00176
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An electrochemical intramolecular oxytrifluorome-thylation of N-tethered alkenyl alcohols was developed providing straightforward access to CF3-containing morpholines derivatives. The method features mild reaction conditions with direct anodic oxidation of Langlois reagent as a cheap and easy to handle trifluoromethylating reagent. Variously substituted 2-(2,2,2-trifluoroethyl)morpholines were obtained in moderate to high yields under constant current electrolysis in an undivided cell.
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