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Mechanical, rheological, and stability performance of simulated in-situ cured oil well cement slurries reinforced with alumina nanofibers

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DOI: 10.1016/j.petrol.2019.106415

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Alumina nanofiber (ANF); Mechanical properties; Rheological properties; Oil and gas well cement

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Effects of highly dispersed Alumina Nanofibers (ANF) on the mechanical, rheological, and stability performances in oil well cement were investigated in this study. The cement sheath possesses a vital role in maintaining zonal isolation in the wellbore, supporting the casing, and preventing external casing corrosion. This research focuses on using ANF to improve these functions. Cement class H composed of various concentrations of ANF, 0.2% cement friction reducer (CFR), and distilled water were used in this experimental study. The nanofiber dosage consisted of 0.1%-0.4% ANF in increments of 0.1% by weight of cementitious materials. The nanomaterials were dispersed at various times using an ultrasonic batch to ensure uniform dispersion in the cement class H matrix. A pre-dispersed version was also provided. The most highly dispersed solution was used in all the cement test analysis. The results indicate the pre-dispersed solution at 0.1% ANF greatly increased the compressive strength by 28% after 8 h of curing and 50% after 24 h of curing at 82.2 degrees C (180 degrees F) and 34.47 MPa (5000 psi). Conversely, the tensile strength increased by 9% and 53% after 8 h and 24 h curing, at the same temperature and pressure conditions. Lastly, the differences in rheological, stability performance, and thickening time using cement slurries without ANF compared to slurries with ANF proved insignificant.

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