期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 85, 期 5, 页码 3358-3363出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b03155
关键词
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资金
- Natural Science Foundation of China [51974122]
- National Natural Science Foundation of Hunan Province [2019B50214]
A facile and efficient protocol for the synthesis of 3 substituted 5-amino-1,2,4-thiadiazoles has been developed through the electro-oxidative intramolecular dehydrogenative N-S bond formation of imidoyl thioureas. Various 1,2,4-thiadiazole derivatives were synthesized in good to excellent yields with broad substrate scope and excellent functional group tolerance under catalyst- and oxidant-free electrolytic conditions at room temperature.
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