期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 26, 期 12, 页码 2576-2580出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201904528
关键词
ball milling; carbonylation; mechanochemistry; molybdenum hexacarbonyl; real-time monitoring
资金
- RWTH Aachen University
Esters and amides were mechanochemically prepared by palladium-catalyzed carbonylative reactions of aryl iodides by using molybdenum hexacarbonyl as a convenient solid carbonyl source and avoiding a direct handling of gaseous carbon monoxide. Real-time monitoring of the mechanochemical reaction by in situ pressure sensing revealed that CO is rapidly transferred from Mo(CO)(6) to the active catalytic system without significant release of molecular carbon monoxide.
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