期刊
CERAMICS INTERNATIONAL
卷 46, 期 8, 页码 11149-11153出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2020.01.135
关键词
Fe3O4 nanoparticles; Particle sizes; Magnetic cluster; Co-precipitation; Hydrothermal; Effective anisotropy
资金
- Brazilian funding agency FAPITEC-SE (PRONEX)
- Brazilian funding agency CNPq [303910/2015-1, 455970/2014-9]
- Brazilian funding agency Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior - Brasil (CAPES) [001]
In this work, a comparative study of the synthesis and magnetic properties of Fe3O4 nanoparticles obtained by the co-precipitation and hydrothermal methods with the adding of the sucrose as a chelating agent is reported. The analysis of transmission electron microscopy (TEM) show that particles are spherical-like with an average particle size ranging of 3 <= d <= 10 nm. Magnetization measurements as a function of an applied magnetic field and temperature are consistent with a superparamagnetic behavior with small T-B values. The analysis of the MvsH loops measured at T = 2 K and Zero-Field-Cooled and Field-Cooled (ZFC - FC) curves allows us to estimate the average diameter of Fe3O4 nanoparticles. These results are in good agreement with those obtained through X-ray diffraction (XRD) data (by using Scherrer equation and Williamson-Hall plot) and slightly smaller than those estimated using TEM images. Finally, ZFC - FC data are also used to evaluate the effective anisotropy constants, which are similar to those values found in literature considering the average sizes values estimated by different techniques.
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