期刊
SYNTHESIS-STUTTGART
卷 52, 期 5, 页码 755-762出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0039-1690754
关键词
sulfinates; hydrazones; DIPEA; carbonyl compounds; sulfonylhydrazines
资金
- Key Technology Research and Development Program of Shandong [2019GSF108089]
- Natural Science Foundation of Shandong Province [ZR2019MB009]
- National Natural Science Foundation of China [21372054, 21672046]
- Huancui District of Weihai City
A base-promoted direct synthesis of sulfinates from N-sulfonylhydrazones is described. Various N-sulfonylhydrazones, derived from aldehydes and ketones, are converted into the corresponding sulfinates in moderate to good yields. This protocol possesses many advantages such as readily available and stable starting materials, broad substrate scope, and metal-free reaction conditions.
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