期刊
SYNLETT
卷 30, 期 18, 页码 2058-2061出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0039-1690689
关键词
apparatus; powder handling; glycosylation; inert atmosphere; moisture sensitivity
资金
- JSPS KAKENHI [JP18K05462]
- Heiwa Nakajima Foundation (Japan)
- Takeda Science Foundation (Japan)
- Japan International Cultural Exchange Foundation (Japan)
- Nakamura Jishiro Ikueikai Foundation (Japan)
Addition of reactants under an inert atmosphere is a fundamental but extremely important technique in synthetic chemistry. Although this is achievable in many cases by using a glove box or a Schlenk-and-syringe technique, the direct addition of powder (solid) materials without contamination by air or moisture has been difficult, especially in the later stages of a reaction. Here, we offer a simple and small apparatus to realize powder addition with easy handling. Use of this apparatus permitted one-pot glycosylation reactions that required extremely dry conditions to be performed in a highly reproducible manner.
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