期刊
ORGANIC LETTERS
卷 21, 期 23, 页码 9759-9762出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b03950
关键词
-
资金
- Natural Sciences and Engineering Research Council of Canada (NSERC)
- Fonds de recherche du Quebec-Nature et technologies (FRQ-NT)
- Universite Laval
The use of a methanesulfonic acid/triethylamine trihydrofluoride combination for the direct hydrofluorination of methallyl-containing substrates is reported. Under those metal-free conditions that use readily available, cheap, and easy to handle reagents, a range of methallyl alkenes could be converted to their corresponding tertiary fluoride in up to 78% yield. Finally, a promising result for the adaptation of this chemistry to continuous flow conditions is reported.
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