期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 84, 期 24, 页码 16262-16267出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b02866
关键词
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资金
- Natural Science Foundation of China [51974122]
- Natural Science Foundation of Hunan Province [2019JJ50214]
I-2/dimethyl sulfoxide (DMSO)-mediated C-S, S-N, and C-N bond cross-coupling cyclization reaction for the synthesis of 5-acyl-1,2,3-thiadiazoles from enaminones, tosylhydrazine, and elemental sulfur has been developed under transition-metal-free conditions. This strategy is operationally simple, compatible with a wide range of functional groups, and provides the desired products in moderate to excellent yields.
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