期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 84, 期 22, 页码 14949-14956出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.9b02301
关键词
-
资金
- Science and Technology Planning Project of Guangdong Province [2017A010103044]
- 100 Young Talents Programme of Guangdong University of Technology [220413506]
- Open Fund of the Key Laboratory of Functional Molecular Engineering of Guangdong Province [2016107]
- (South China University of Technology)
A direct and practical metal-free N-H phosphorylation has been achieved via the TBHP/NH4-Imediated cross-dehydrogenative coupling (CDC) reactions between imines/imidates and P(O)H compounds. This transformation provides an efficient synthetic route to the construction of P-N bonds with good functional group compatibility, leading to the formation of N-phosphorylimines and N-phosphorylimidates in up to 95% yield (33 examples) under mild conditions.
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