4.5 Article

Visible-Light-Mediated C(sp3)-H Thiocarbonylation for Thiolactam Preparation with Potassium Sulfide

期刊

CHINESE JOURNAL OF CHEMISTRY
卷 37, 期 12, 页码 1234-1238

出版社

WILEY-V C H VERLAG GMBH
DOI: 10.1002/cjoc.201900360

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资金

  1. National Key Research and Development Program of China [2017YFD0200500]
  2. NSFC [21971065, 21722202, 21672069]
  3. S&TCSM of Shanghai [18JC1415600]
  4. Shanghai Institutions of Higher Learning
  5. National Program for Support of Top-notch Young Professionals

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The Summary of main observation and conclusion We report herein a protocol for thiolactam preparation with potassium sulfide via visible-light-mediated C(sp(3))-H thiocarbonylation, in which polysulfide dianions and radical anions generated from potassium sulfide were the key active species. A variety of thiolactams were straightforward established under mild conditions. Moreover, it was successfully applied to structural modification of tetrahydroberberine.

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