期刊
CHINESE JOURNAL OF CHEMISTRY
卷 37, 期 12, 页码 1234-1238出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cjoc.201900360
关键词
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资金
- National Key Research and Development Program of China [2017YFD0200500]
- NSFC [21971065, 21722202, 21672069]
- S&TCSM of Shanghai [18JC1415600]
- Shanghai Institutions of Higher Learning
- National Program for Support of Top-notch Young Professionals
The Summary of main observation and conclusion We report herein a protocol for thiolactam preparation with potassium sulfide via visible-light-mediated C(sp(3))-H thiocarbonylation, in which polysulfide dianions and radical anions generated from potassium sulfide were the key active species. A variety of thiolactams were straightforward established under mild conditions. Moreover, it was successfully applied to structural modification of tetrahydroberberine.
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