期刊
ANALYTICAL CHEMISTRY
卷 91, 期 24, 页码 15355-15359出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.analchem.9b04316
关键词
-
资金
- National Science Foundation [CHE-1763337, CHE-1900401]
- U.S. DOE Office of Science Facility, at Brookhaven National Laboratory [DE-SC0012704]
High-resolution scanning electrochemical microscopy (SECM) is a powerful technique for mapping surface topography and reactivity on the nanoscale and investigating heterogeneous processes at the level of single nanoparticles. The ability to fabricate ultrasmall nanoelectrode tips is critical for the progress in nano-SECM. Despite long-term efforts to improve previously developed procedures, the preparation and characterization of disk-type polished tips with the radius
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