期刊
JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
卷 28, 期 10, 页码 6287-6297出版社
SPRINGER
DOI: 10.1007/s11665-019-04336-0
关键词
B4C/6061Al nanocomposites; constitutive equation; hot deformation; processing map; spark plasma sintering
资金
- National Natural Science Foundation of China, China [51505320, 51805358]
- Key Science and Technology Program of Shanxi Province, China [20130321024]
We developed 3 vol.% B4C/6061Al nanocomposites by spark plasma sintering. We then characterized their flow and hot deformation behaviors using isothermal compression tests at deformation temperatures of 673-823 K and strain rates of 0.001-1 s(-1). Results indicated that their steady flow characteristic can be described by the Zener-Hollomon parameter (Z) as a hyperbolic-sine function of flow stress. Based on pinning effect from B4C nanoparticles, the estimated activation energy was calculated to be 274.80 kJ/mol. At the unstable deformation condition (723 K/1 s(-1)) with high Z, flow localization appeared; the main softening mechanisms involved are dynamic recovery and dynamic recrystallization (DRX). At the stable deformation condition (823 K/0.001 s(-1)) with low Z, adequate DRX occurred. Based on the processing map and microstructure evolution, the optimum hot working conditions for B4C/6061Al nanocomposites were determined to be a deformation temperature of 773-823 K and a strain rate of 0.001-0.003 s(-1). These working conditions were verified by a hot extrusion test.
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