期刊
JOURNAL OF ALLOYS AND COMPOUNDS
卷 801, 期 -, 页码 40-48出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2019.06.110
关键词
Graphene oxide; Electro-brush plating; Composite coatings; Microstructure; Mechanical properties
资金
- National Natural Science Foundation of China [51775127, 51575118]
- National Basic Research Program of China (973 Program) [61328303]
- Marine Low Speed Engine Project-Phase I [CDGC01-KT0302]
- Natural Science Foundation of Heilongjiang Province [E2018020]
- Fundamental Research Funds for the Central Universities [3072019CF1010]
Enhancement of mechanical performances is a challenging issue for Fe-based coatings prepared by electro-brush plating technique (EBP), and graphene oxide (GO) has been regarded as a promising additive currently. Thus, in this work, GO sheets were used to improve the microstructure and mechanical properties of electro-brush plated Fe coatings. The results showed that GO was reduced to the reduced graphene oxide (rGO) undergoing the electrochemical reduction, and the rGO sheets were co-deposited with those metal atoms during EBP. As expected, the defects number of Fe coatings was decreased obviously with the addition of GO, which is attributed to that the co-deposition process of GO with Fe atoms could facilitate the emission of hydrogen atoms away from the cathode, avoiding the formation of hydrogen-induced defects in coatings. In addition, the grains of Fe-GO composite coatings were remarkably refined as the rGO sheets provided heterogeneous nucleation sites for the primary Fe crystals. Improved micro-hardness and wear resistance were achieved after adding GO. Compared with Fe coatings, the average friction coefficient and weight loss of Fe-GO composite coatings were decreased by 49.5% and 39.7%, respectively, due to the effect of self-lubrication and reinforcement of rGO sheets. (C) 2019 Elsevier B.V. All rights reserved.
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