期刊
ORGANIC LETTERS
卷 21, 期 13, 页码 5132-5137出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.9b01730
关键词
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资金
- ANR (CarNuCat) [ANR-15-CE29- 0002]
- la Ligue Contre le Cancer through an Equipe Labellisee 2014 grant
- China Scholarship Council
- Laboratory of Excellence CHARMMMAT
- CNRS
- University Paris-Sud
- [ANR-10-LABX-33]
- Agence Nationale de la Recherche (ANR) [ANR-15-CE29-0002] Funding Source: Agence Nationale de la Recherche (ANR)
A general protocol for functionalization of glycosyl thiols has been reported. This protocol is based on a single-electron Ni/photoredox dual-catalyzed cross coupling between 1-thiosugars and a broad range of aryl bromides and iodides as well as alkenyl and alkynyl halides. This base-free method gives access to a series of functionalized thioglycosides in moderate to excellent yields with a perfect control of the anomeric configuration. Moreover, it has been shown that this methodology may be transposed successfully to the continuous-flow photoredox chemistry.
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