期刊
MICROSCOPY AND MICROANALYSIS
卷 25, 期 6, 页码 1449-1456出版社
CAMBRIDGE UNIV PRESS
DOI: 10.1017/S1431927619014648
关键词
energy dispersive X-ray spectroscopy (EDS); molybdenum oxide (MoO3); noble metal (Ag; Au); scanning electron microscopy (SEM)
We report the growth of molybdenum trioxide (MoO3) nanoribbons (NRs) on epitaxial Ag and oriented Au nanostructures (NSs) using an ultra-high vacuum (UHV)-molecular beam epitaxy (MBE) technique at different substrate temperatures. An approximately 2 nm silver (Ag) film has been deposited at different growth temperatures (using UHV-MBE) on cleaned Si(100), Si(110), and Si(111) substrates. For faceted Au NSs, an approximately 50 nm Au film has been deposited (using high-vacuum thermal evaporation) on a Si(100) substrate with a native oxide layer at the interface and the sample was annealed in low vacuum (approximate to 10(-2)) and at high temperature (approximate to 975 degrees C). Scanning electron microscopy measurements were performed to determine the morphology of MoO3/Ag and MoO3/Au composite films. From energy dispersive X-ray spectroscopy elemental mapping and line scans it is found that faceted Au NSs are more favorable for the growth of MoO3 NRs than epitaxial Ag microstructures.
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