期刊
APPLIED SURFACE SCIENCE
卷 380, 期 -, 页码 193-202出版社
ELSEVIER
DOI: 10.1016/j.apsusc.2016.01.204
关键词
Inert Gas Condensation; TiO2 nanoflowers; Cu nanoclusters; SnO2 nanoparticles
Sn and Cu oxide nanoparticles were deposited by Inert Gas Condensation (IGC) technique combined with dc magnetron sputtering onto nanoflower TiO2 3D substrates obtained in the oxidation process of Ti-foil in 30% H2O2. Sputtering parameters such as insertion length and Ar/He flow rates were optimized taking into account the nanostructure morphology. Comparative studies with hydrothermal method were carried out. Surface properties of the synthesized nanomaterials were studied by Scanning Electron Microscopy, SEM, Atomic Force Microscopy, AFM, and X-ray Photoelectron Spectroscopy, XPS. X-ray diffraction, XRD and Raman spectroscopy were performed in order to determine phase composition. Impedance spectroscopy demonstrated the influence of nanoparticles on the electrical conductivity. (C) 2016 Elsevier B.V. All rights reserved.
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